TA Instruments

AR1741-0004f

15/03/2013 11:17:23

Sample name	ASW Blank coupon#23
Sample notes	 
Experiment notes	ASW Articial Sea Water, 25 mm diameter. 70 mm depth of water, 10 mm gap
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1741
Run number	4 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 11:17:23

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	4.850	-121.78	10000	22.4	5.681E-3	31.004	-39.69	6.063	-6.547	23.15	2.3957	0.6297	2.9946	299.46	3.383E-3	0.0	0.5
2.0080	10.23	2.8470	10000	22.4	4.869E-3	32.008	0.9280	12.78	0.07259	19.84	13.9436	0.1214	17.430	1743.0	3.384E-3	0.0	0.5
3.0040	15.68	5.1333	10000	22.4	6.898E-3	33.004	1.673	19.60	0.08539	28.11	27.8076	0.07320	34.760	3476.0	3.383E-3	0.1	0.6
4.0160	18.57	6.8817	10000	22.4	8.319E-3	34.016	2.243	23.22	0.09662	33.89	41.3123	0.06289	51.640	5164.0	3.384E-3	0.1	0.6
5.0200	24.77	10.689	10000	22.4	0.01116	35.020	3.484	30.96	0.1125	45.47	68.0499	0.04742	85.062	8506.2	3.384E-3	0.1	0.6
6.0040	31.66	16.330	10000	22.4	4.666E-3	36.004	5.323	39.58	0.1345	19.01	107.3150	0.01214	134.14	13414	3.384E-3	0.1	0.6
7.0160	34.10	18.460	10000	22.4	4.261E-3	37.016	6.017	42.62	0.1412	17.36	126.7740	9.556E-3	158.47	15847	3.383E-3	0.1	0.6
8.0840	41.73	25.751	10000	22.4	5.681E-3	38.084	8.394	52.16	0.1609	23.15	185.1050	8.506E-3	231.38	23138	3.384E-3	0.1	0.6
9.0040	46.08	30.125	10000	22.4	6.087E-3	39.004	9.819	57.60	0.1705	24.80	223.6190	7.475E-3	279.52	27952	3.383E-3	0.2	0.7
10.004	51.00	36.753	10000	22.4	4.058E-3	40.004	11.98	63.75	0.1879	16.53	275.1660	4.069E-3	343.96	34396	3.384E-3	0.2	0.7
11.004	55.76	42.789	10000	22.4	4.261E-3	41.004	13.95	69.70	0.2001	17.36	326.5100	3.573E-3	408.14	40814	3.383E-3	0.2	0.7
12.016	60.13	48.431	10000	22.4	3.043E-3	42.016	15.79	75.17	0.2100	12.40	377.6370	2.195E-3	472.05	47205	3.383E-3	0.2	0.7
13.000	64.45	54.016	10000	22.4	2.840E-3	43.000	17.61	80.56	0.2186	11.57	435.8790	1.783E-3	544.85	54485	3.383E-3	0.2	0.7
14.004	69.18	60.353	10000	22.4	-1.420E-3	44.004	19.67	86.47	0.2275	-5.787	499.0460	-7.739E-4	623.81	62381	3.383E-3	0.2	0.7
15.060	75.71	69.931	10000	22.4	-4.058E-4	45.060	22.79	94.64	0.2409	-1.653	594.6600	-1.846E-4	743.33	74333	3.383E-3	0.3	0.8
16.004	79.96	76.952	10000	22.4	6.087E-4	46.004	25.08	99.94	0.2510	2.480	665.4290	2.483E-4	831.79	83179	3.383E-3	0.3	0.8
17.008	84.55	83.430	10000	22.4	-2.840E-3	47.008	27.19	105.7	0.2573	-11.57	741.0550	-1.036E-3	926.32	92632	3.383E-3	0.3	0.8
18.020	91.01	93.125	10000	22.4	-4.261E-3	48.020	30.35	113.8	0.2668	-17.36	855.8560	-1.341E-3	1069.8	1.0698E5	3.383E-3	0.3	0.8
19.004	95.06	100.76	10000	22.4	-3.043E-3	49.004	32.84	118.8	0.2764	-12.40	932.1750	-8.782E-4	1165.2	1.1652E5	3.383E-3	0.3	0.8
20.004	99.42	110.22	10000	22.4	-5.072E-3	50.004	35.93	124.3	0.2891	-20.67	1020.5600	-1.338E-3	1275.7	1.2757E5	3.383E-3	0.3	0.8
21.004	105.8	120.85	10000	22.4	-5.884E-3	51.004	39.39	132.3	0.2977	-23.97	1153.7500	-1.369E-3	1442.2	1.4422E5	3.383E-3	0.4	0.9
22.008	109.9	128.11	10000	22.4	-6.087E-3	52.008	41.76	137.4	0.3039	-24.80	1243.0699	-1.314E-3	1553.8	1.5538E5	3.384E-3	0.4	0.9
23.004	114.3	135.52	10000	22.4	-4.869E-3	53.004	44.17	142.8	0.3093	-19.84	1344.0100	-9.726E-4	1680.0	1.6800E5	3.383E-3	0.4	0.9
24.072	120.7	149.11	10000	22.4	-7.101E-3	54.072	48.60	150.8	0.3222	-28.93	1496.0900	-1.272E-3	1870.1	1.8701E5	3.383E-3	0.4	0.9
25.000	124.8	157.61	10000	22.4	-4.058E-3	55.000	51.37	155.9	0.3294	-16.53	1598.5000	-6.799E-4	1998.1	1.9981E5	3.383E-3	0.4	0.9
26.000	129.1	166.88	10000	22.4	-0.01035	56.000	54.40	161.3	0.3371	-42.16	1711.3700	-1.620E-3	2139.2	2.1392E5	3.383E-3	0.4	0.9
27.004	135.5	182.77	10000	22.4	-0.01136	57.004	59.58	169.3	0.3518	-46.29	1882.3600	-1.614E-3	2353.0	2.3530E5	3.383E-3	0.5	1.0
28.000	139.6	190.90	10000	22.4	-0.01075	58.000	62.22	174.5	0.3567	-43.81	1996.8500	-1.439E-3	2496.1	2.4961E5	3.384E-3	0.5	1.0
28.996	143.7	198.01	10000	22.4	-0.01116	58.996	64.54	179.6	0.3594	-45.47	2116.4800	-1.410E-3	2645.6	2.6456E5	3.384E-3	0.5	1.0
30.004	150.1	213.73	10000	22.4	-9.942E-3	60.004	69.67	187.6	0.3714	-40.51	2306.2100	-1.151E-3	2882.8	2.8828E5	3.384E-3	0.5	1.0
31.004	154.2	222.31	10000	22.4	-0.01278	61.004	72.46	192.7	0.3760	-52.08	2432.6499	-1.402E-3	3040.8	3.0408E5	3.383E-3	0.5	1.0
31.996	158.3	232.02	10000	22.4	-0.01684	61.996	75.63	197.8	0.3823	-68.61	2566.0901	-1.753E-3	3207.6	3.2076E5	3.383E-3	0.5	1.0
33.000	164.7	249.18	10000	22.4	-0.01522	63.000	81.22	205.8	0.3946	-62.00	2774.1201	-1.463E-3	3467.7	3.4677E5	3.384E-3	0.6	1.1
33.996	168.8	254.36	10000	22.4	-0.01420	63.996	82.91	211.0	0.3929	-57.87	2913.1001	-1.300E-3	3641.4	3.6414E5	3.384E-3	0.6	1.1
35.000	174.9	272.99	10000	22.4	-0.01684	65.000	88.98	218.6	0.4070	-68.61	3128.0100	-1.436E-3	3910.0	3.9100E5	3.384E-3	0.6	1.1
36.004	179.1	283.98	10000	22.4	-0.02313	66.004	92.56	223.9	0.4134	-94.24	3292.3401	-1.880E-3	4115.4	4.1154E5	3.383E-3	0.6	1.1
37.000	183.3	297.12	10000	22.4	-0.01806	67.000	96.85	229.1	0.4227	-73.57	3432.8401	-1.402E-3	4291.1	4.2911E5	3.384E-3	0.6	1.1
38.216	189.3	308.98	10000	22.4	-0.02029	68.216	100.7	236.6	0.4256	-82.67	3658.8201	-1.476E-3	4573.5	4.5735E5	3.384E-3	0.6	1.1
39.000	193.5	319.36	10000	22.4	-0.01907	69.000	104.1	241.8	0.4304	-77.71	3822.5000	-1.329E-3	4778.1	4.7781E5	3.384E-3	0.7	1.2
40.004	199.7	330.23	10000	22.4	-0.02333	70.004	107.6	249.6	0.4312	-95.07	4068.8000	-1.526E-3	5086.0	5.0860E5	3.384E-3	0.7	1.2
41.020	203.8	335.95	10000	22.4	-0.02272	71.020	109.5	254.7	0.4299	-92.59	4233.9199	-1.427E-3	5292.4	5.2924E5	3.384E-3	0.7	1.2
42.000	207.9	353.18	10000	22.4	-0.02577	72.000	115.1	259.9	0.4430	-105.0	4409.7202	-1.555E-3	5512.2	5.5122E5	3.384E-3	0.7	1.2
43.000	214.1	368.45	10000	22.4	-0.02496	73.000	120.1	267.6	0.4487	-101.7	4676.1699	-1.420E-3	5845.2	5.8452E5	3.384E-3	0.7	1.2
44.004	218.1	386.30	10000	22.4	-0.02577	74.004	125.9	272.7	0.4618	-105.0	4851.5000	-1.412E-3	6064.4	6.0644E5	3.384E-3	0.7	1.2
45.004	224.3	395.19	10000	22.4	-0.02698	75.004	128.8	280.4	0.4595	-109.9	5129.2798	-1.399E-3	6411.6	6.4116E5	3.384E-3	0.8	1.3
46.000	228.4	416.22	10000	22.4	-0.03003	76.000	135.7	285.5	0.4751	-122.3	5318.4199	-1.501E-3	6648.0	6.6480E5	3.384E-3	0.8	1.3
47.000	234.5	429.64	10000	22.4	-0.02800	77.000	140.0	293.1	0.4777	-114.1	5602.3701	-1.328E-3	7003.0	7.0030E5	3.384E-3	0.8	1.3
48.000	238.5	451.84	10000	22.4	-0.03246	78.000	147.3	298.1	0.4940	-132.3	5799.3901	-1.488E-3	7249.2	7.2492E5	3.384E-3	0.8	1.3
49.000	242.7	455.02	10000	22.4	-0.03206	79.000	148.3	303.4	0.4889	-130.6	6000.0298	-1.419E-3	7500.0	7.5000E5	3.384E-3	0.8	1.3
50.016	248.8	475.30	10000	22.4	-0.03185	80.016	154.9	311.0	0.4982	-129.8	6303.8501	-1.342E-3	7879.8	7.8798E5	3.384E-3	0.8	1.3
51.020	252.8	503.69	10000	22.4	-0.03652	81.020	164.2	316.0	0.5195	-148.8	6512.0601	-1.490E-3	8140.1	8.1401E5	3.384E-3	0.9	1.4
52.000	259.0	499.13	10000	22.4	-0.03591	82.000	162.7	323.8	0.5024	-146.3	6832.3198	-1.395E-3	8540.4	8.5404E5	3.384E-3	0.9	1.4
52.996	263.1	522.47	10000	22.4	-0.03591	82.996	170.3	328.9	0.5178	-146.3	7046.8101	-1.352E-3	8808.5	8.8085E5	3.384E-3	0.9	1.4
54.020	269.2	545.19	10000	22.4	-0.04058	84.020	177.7	336.5	0.5281	-165.3	7376.5601	-1.460E-3	9220.7	9.2207E5	3.384E-3	0.9	1.4
54.996	273.3	555.68	10000	22.4	-0.04585	84.996	181.1	341.6	0.5302	-186.8	7602.9502	-1.601E-3	9503.7	9.5037E5	3.383E-3	0.9	1.4
56.000	277.4	555.35	10000	22.4	-0.04301	86.000	181.0	346.7	0.5221	-175.3	7828.6401	-1.458E-3	9785.8	9.7858E5	3.384E-3	0.9	1.4
57.004	283.4	607.26	10000	22.4	-0.04545	87.004	197.9	354.2	0.5588	-185.2	8169.7900	-1.476E-3	10212	1.0212E6	3.384E-3	1.0	1.5
57.996	287.5	614.01	10000	22.4	-0.04748	87.996	200.1	359.3	0.5570	-193.4	8410.8799	-1.498E-3	10514	1.0514E6	3.384E-3	1.0	1.5
58.996	293.6	621.80	10000	22.4	-0.05113	88.996	202.7	367.0	0.5523	-208.3	8767.9902	-1.547E-3	10960	1.0960E6	3.384E-3	1.0	1.5
60.016	297.6	647.24	10000	22.4	-0.04524	90.016	211.0	372.0	0.5671	-184.3	9007.6396	-1.332E-3	11260	1.1260E6	3.384E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	300.0	647.59	10000	22.4	-0.05072	91.996	211.1	375.0	0.5628	-206.7	303.9110	-1.469E-3	379.89	37989	3.384E-3	0.0	1.5
2.0120	300.0	639.12	10000	22.4	-0.05356	93.012	208.3	375.1	0.5554	-218.2	556.6590	-1.551E-3	695.82	69582	3.384E-3	0.0	1.6
3.0120	300.0	653.26	10000	22.4	-0.04342	94.012	212.9	375.0	0.5679	-176.9	807.9620	-1.258E-3	1010.0	1.0100E5	3.384E-3	0.1	1.6
3.9960	300.0	663.10	10000	22.4	-0.04606	94.996	216.1	375.0	0.5764	-187.6	1186.2200	-1.335E-3	1482.8	1.4828E5	3.384E-3	0.1	1.6
5.0080	300.0	641.81	10000	22.4	-0.05823	96.008	209.2	375.0	0.5578	-237.2	1436.3800	-1.687E-3	1795.5	1.7955E5	3.384E-3	0.1	1.6
6.0160	300.0	660.30	10000	22.4	-0.04301	97.016	215.2	375.0	0.5739	-175.3	1813.1300	-1.246E-3	2266.4	2.2664E5	3.384E-3	0.1	1.6
7.0120	300.0	649.51	10000	22.4	-0.05377	98.012	211.7	375.0	0.5646	-219.1	2062.8401	-1.558E-3	2578.6	2.5786E5	3.384E-3	0.1	1.6
8.0120	300.0	632.64	10000	22.4	-0.04058	99.012	206.2	375.0	0.5499	-165.3	2314.9099	-1.176E-3	2893.6	2.8936E5	3.384E-3	0.1	1.7
9.0120	300.0	655.46	10000	22.4	-0.05235	100.012	213.6	374.9	0.5698	-213.3	2691.1299	-1.517E-3	3363.9	3.3639E5	3.384E-3	0.2	1.7
9.9920	300.0	642.22	10000	22.4	-0.04200	100.992	209.3	375.0	0.5582	-171.1	2944.9299	-1.217E-3	3681.2	3.6812E5	3.383E-3	0.2	1.7
10.996	300.0	652.25	10000	22.4	-0.04423	101.996	212.6	375.0	0.5670	-180.2	3320.5901	-1.282E-3	4150.7	4.1507E5	3.383E-3	0.2	1.7
12.016	299.9	693.94	10000	22.4	-0.05113	103.016	226.2	374.9	0.6033	-208.3	3571.6699	-1.482E-3	4464.6	4.4646E5	3.384E-3	0.2	1.7
13.016	300.0	646.42	10000	22.4	-0.04748	104.016	210.7	375.0	0.5619	-193.4	3822.1499	-1.376E-3	4777.7	4.7777E5	3.384E-3	0.2	1.7
14.012	300.0	639.34	10000	22.4	-0.04524	105.012	208.4	375.0	0.5557	-184.3	4199.1201	-1.311E-3	5248.9	5.2489E5	3.384E-3	0.2	1.8
15.012	300.1	623.50	10000	22.4	-0.05194	106.012	203.2	375.1	0.5418	-211.6	4450.3799	-1.504E-3	5563.0	5.5630E5	3.383E-3	0.3	1.8
16.012	300.0	649.26	10000	22.4	-0.05295	107.012	211.6	375.0	0.5644	-215.8	4701.7300	-1.535E-3	5877.2	5.8772E5	3.383E-3	0.3	1.8
17.012	300.0	650.57	10000	22.4	-0.04606	108.012	212.1	375.0	0.5654	-187.6	5078.8501	-1.334E-3	6348.6	6.3486E5	3.383E-3	0.3	1.8
18.016	300.0	672.93	10000	22.4	-0.04078	109.016	219.3	375.0	0.5849	-166.2	5330.0801	-1.182E-3	6662.6	6.6626E5	3.383E-3	0.3	1.8
19.012	300.0	647.49	10000	22.4	-0.04748	110.012	211.1	375.0	0.5628	-193.4	5707.2002	-1.375E-3	7134.0	7.1340E5	3.384E-3	0.3	1.8
20.012	300.0	631.51	10000	22.4	-0.05153	111.012	205.8	375.1	0.5488	-210.0	5958.5000	-1.493E-3	7448.1	7.4481E5	3.384E-3	0.3	1.9
21.016	300.0	642.94	10000	22.4	-0.04159	112.016	209.6	375.0	0.5588	-169.5	6209.6899	-1.205E-3	7762.1	7.7621E5	3.384E-3	0.4	1.9
22.012	300.0	639.21	10000	22.4	-0.04707	113.012	208.3	375.0	0.5556	-191.8	6586.6899	-1.364E-3	8233.4	8.2334E5	3.384E-3	0.4	1.9
23.012	300.0	649.80	10000	22.4	-0.05620	114.012	211.8	375.0	0.5648	-229.0	6840.6299	-1.628E-3	8550.8	8.5508E5	3.384E-3	0.4	1.9
24.016	300.0	657.91	10000	22.4	-0.05052	115.016	214.4	375.0	0.5719	-205.8	7215.1401	-1.464E-3	9018.9	9.0189E5	3.384E-3	0.4	1.9
25.000	300.0	652.55	10000	22.4	-0.04565	116.000	212.7	375.0	0.5672	-186.0	7466.4800	-1.323E-3	9333.1	9.3331E5	3.383E-3	0.4	1.9
26.016	300.1	652.66	10000	22.4	-0.05194	117.016	212.7	375.1	0.5672	-211.6	7717.8501	-1.504E-3	9647.3	9.6473E5	3.384E-3	0.4	2.0
27.016	300.0	658.83	10000	22.4	-0.04484	118.016	214.7	375.0	0.5726	-182.7	8094.7002	-1.299E-3	10118	1.0118E6	3.384E-3	0.5	2.0
28.012	300.0	654.88	10000	22.4	-0.04727	119.012	213.5	375.0	0.5693	-192.6	8345.9297	-1.370E-3	10432	1.0432E6	3.384E-3	0.5	2.0
29.012	300.0	632.09	10000	22.4	-0.05153	120.012	206.0	375.0	0.5494	-210.0	8726.0303	-1.493E-3	10908	1.0908E6	3.384E-3	0.5	2.0
29.996	300.0	651.17	10000	22.4	-0.04585	120.996	212.2	375.0	0.5660	-186.8	8974.2598	-1.329E-3	11218	1.1218E6	3.384E-3	0.5	2.0

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0000	296.1	626.23	10000	22.4	-0.04362	122.000	204.1	370.1	0.5515	-177.7	328.8540	-1.297E-3	411.07	41107	3.383E-3	0.0	2.0
2.0120	292.1	607.94	10000	22.4	-0.04342	123.012	198.2	365.1	0.5427	-176.9	567.9070	-1.327E-3	709.88	70988	3.384E-3	0.0	2.1
3.0120	288.0	580.95	10000	22.4	-0.03490	124.012	189.4	360.1	0.5259	-142.2	804.6000	-1.097E-3	1005.8	1.0058E5	3.384E-3	0.1	2.1
3.9960	281.9	590.57	10000	22.4	-0.04626	124.996	192.5	352.3	0.5464	-188.5	1163.4900	-1.518E-3	1454.4	1.4544E5	3.384E-3	0.1	2.1
4.9960	277.8	569.01	10000	22.4	-0.03936	125.996	185.5	347.3	0.5340	-160.4	1387.0200	-1.330E-3	1733.8	1.7338E5	3.384E-3	0.1	2.1
6.0160	271.7	563.13	10000	22.4	-0.04139	127.016	183.6	339.6	0.5405	-168.6	1727.5000	-1.462E-3	2159.4	2.1594E5	3.384E-3	0.1	2.1
6.9960	267.6	544.45	10000	22.4	-0.03713	127.996	177.5	334.4	0.5306	-151.3	1951.4600	-1.352E-3	2439.3	2.4393E5	3.384E-3	0.1	2.1
8.0120	261.5	531.06	10000	22.4	-0.03896	129.012	173.1	326.9	0.5296	-158.7	2269.7000	-1.486E-3	2837.1	2.8371E5	3.384E-3	0.1	2.2
9.0120	257.5	506.31	10000	22.4	-0.03591	130.012	165.0	321.8	0.5128	-146.3	2482.6201	-1.413E-3	3103.3	3.1033E5	3.384E-3	0.2	2.2
10.000	253.3	497.19	10000	22.4	-0.03571	131.000	162.1	316.7	0.5118	-145.5	2695.3799	-1.451E-3	3369.2	3.3692E5	3.384E-3	0.2	2.2
10.996	247.2	475.59	10000	22.4	-0.03611	131.996	155.0	309.0	0.5017	-147.1	3011.9099	-1.541E-3	3764.9	3.7649E5	3.384E-3	0.2	2.2
11.996	243.2	471.06	10000	22.4	-0.03469	132.996	153.5	303.9	0.5052	-141.4	3202.5901	-1.530E-3	4003.2	4.0032E5	3.384E-3	0.2	2.2
12.996	237.0	442.33	10000	22.4	-0.02861	133.996	144.2	296.2	0.4867	-116.6	3505.7700	-1.328E-3	4382.2	4.3822E5	3.383E-3	0.2	2.2
14.012	232.8	432.68	10000	22.4	-0.03632	135.012	141.0	291.0	0.4846	-148.0	3697.4500	-1.747E-3	4621.8	4.6218E5	3.384E-3	0.2	2.3
15.016	226.8	414.89	10000	22.4	-0.03023	136.016	135.2	283.5	0.4771	-123.2	3978.7000	-1.533E-3	4973.4	4.9734E5	3.384E-3	0.3	2.3
15.996	222.6	399.20	10000	22.4	-0.02942	136.996	130.1	278.3	0.4676	-119.9	4167.6802	-1.548E-3	5209.6	5.2096E5	3.384E-3	0.3	2.3
16.992	218.5	399.86	10000	22.4	-0.02597	137.992	130.3	273.1	0.4772	-105.8	4347.4399	-1.419E-3	5434.3	5.4343E5	3.383E-3	0.3	2.3
18.012	212.4	379.33	10000	22.4	-0.02719	139.012	123.6	265.6	0.4656	-110.8	4610.7500	-1.571E-3	5763.4	5.7634E5	3.383E-3	0.3	2.3
18.996	208.4	353.74	10000	22.4	-0.02435	139.996	115.3	260.4	0.4427	-99.20	4785.2998	-1.462E-3	5981.6	5.9816E5	3.383E-3	0.3	2.3
20.016	202.0	358.77	10000	22.4	-0.02029	141.016	116.9	252.5	0.4630	-82.67	5041.6499	-1.296E-3	6302.1	6.3021E5	3.383E-3	0.3	2.4
21.020	198.1	328.29	10000	22.4	-0.02475	142.020	107.0	247.6	0.4322	-100.9	5205.3301	-1.645E-3	6506.7	6.5067E5	3.383E-3	0.4	2.4
21.996	193.9	325.95	10000	22.4	-0.02577	142.996	106.2	242.4	0.4383	-105.0	5367.9399	-1.787E-3	6709.9	6.7099E5	3.383E-3	0.4	2.4
23.012	187.6	304.22	10000	22.4	-0.01785	144.012	99.16	234.5	0.4228	-72.75	5610.4502	-1.323E-3	7013.1	7.0131E5	3.383E-3	0.4	2.4
24.012	183.5	296.49	10000	22.4	-0.01806	145.012	96.64	229.4	0.4213	-73.57	5760.6602	-1.398E-3	7200.8	7.2008E5	3.383E-3	0.4	2.4
24.992	177.3	279.44	10000	22.4	-0.01522	145.992	91.08	221.7	0.4109	-62.00	5986.9600	-1.262E-3	7483.7	7.4837E5	3.383E-3	0.4	2.4
25.996	173.1	272.73	10000	22.4	-0.01461	146.996	88.90	216.4	0.4108	-59.52	6137.8101	-1.271E-3	7672.3	7.6723E5	3.383E-3	0.4	2.4
27.000	169.0	256.96	10000	22.4	-0.01278	148.000	83.76	211.3	0.3964	-52.08	6272.8901	-1.166E-3	7841.1	7.8411E5	3.384E-3	0.5	2.5
27.996	162.9	245.84	10000	22.4	-0.01501	148.996	80.13	203.6	0.3935	-61.17	6479.0898	-1.475E-3	8098.9	8.0989E5	3.384E-3	0.5	2.5
29.008	158.7	232.88	10000	22.4	-9.942E-3	150.008	75.91	198.3	0.3827	-40.51	6616.3701	-1.030E-3	8270.5	8.2705E5	3.384E-3	0.5	2.5
30.016	154.4	221.89	10000	22.4	-9.130E-3	151.016	72.33	193.0	0.3747	-37.20	6811.2202	-9.984E-4	8514.0	8.5140E5	3.384E-3	0.5	2.5
31.016	148.3	207.70	10000	22.4	-2.638E-3	152.016	67.70	185.4	0.3652	-10.75	6935.6099	-3.128E-4	8669.5	8.6695E5	3.383E-3	0.5	2.5
31.996	144.1	199.87	10000	22.4	-5.681E-3	152.996	65.15	180.1	0.3618	-23.15	7061.1602	-7.138E-4	8826.5	8.8265E5	3.383E-3	0.5	2.5
33.012	137.8	185.24	10000	22.4	-7.507E-3	154.012	60.38	172.3	0.3505	-30.59	7234.2998	-1.031E-3	9042.9	9.0429E5	3.384E-3	0.6	2.6
33.992	133.7	177.37	10000	22.4	-5.681E-3	154.992	57.81	167.1	0.3459	-23.15	7347.7500	-8.285E-4	9184.7	9.1847E5	3.384E-3	0.6	2.6
35.008	129.5	166.50	10000	22.4	-2.638E-3	156.008	54.27	161.9	0.3353	-10.75	7458.9102	-4.102E-4	9323.6	9.3236E5	3.384E-3	0.6	2.6
35.996	123.0	154.39	10000	22.4	-3.855E-3	156.996	50.32	153.8	0.3273	-15.71	7620.8901	-6.642E-4	9526.1	9.5261E5	3.383E-3	0.6	2.6
37.012	118.9	147.42	10000	22.4	-3.449E-3	158.012	48.05	148.7	0.3232	-14.05	7720.6299	-6.358E-4	9650.8	9.6508E5	3.383E-3	0.6	2.6
37.996	114.7	139.73	10000	22.4	-1.623E-3	158.996	45.55	143.4	0.3176	-6.613	7823.4302	-3.216E-4	9779.3	9.7793E5	3.384E-3	0.6	2.6
39.012	108.2	127.60	10000	22.4	3.246E-3	160.012	41.59	135.3	0.3075	13.23	7963.5601	7.229E-4	9954.5	9.9545E5	3.383E-3	0.7	2.7
39.996	104.1	119.89	10000	22.4	-2.029E-4	160.996	39.08	130.2	0.3002	-0.8267	8050.7002	-4.878E-5	10063	1.0063E6	3.384E-3	0.7	2.7
41.012	99.92	112.04	10000	22.4	-4.058E-4	162.012	36.52	124.9	0.2924	-1.653	8139.6899	-1.060E-4	10175	1.0175E6	3.383E-3	0.7	2.7
42.012	93.22	100.01	10000	22.4	-4.058E-4	163.012	32.60	116.5	0.2797	-1.653	8268.7100	-1.218E-4	10336	1.0336E6	3.384E-3	0.7	2.7
43.000	89.00	92.649	10000	22.4	2.029E-4	164.000	30.20	111.3	0.2714	0.8267	8342.9297	6.679E-5	10429	1.0429E6	3.384E-3	0.7	2.7
44.008	84.75	85.174	10000	22.4	5.072E-3	165.008	27.76	105.9	0.2621	20.67	8417.6904	1.841E-3	10522	1.0522E6	3.384E-3	0.7	2.8
45.012	80.28	79.530	10000	22.4	-2.840E-3	166.012	25.92	100.4	0.2583	-11.57	8492.1299	-1.149E-3	10615	1.0615E6	3.384E-3	0.8	2.8
46.020	73.71	68.454	10000	22.4	-8.116E-4	167.020	22.31	92.13	0.2422	-3.307	8591.0098	-3.896E-4	10739	1.0739E6	3.384E-3	0.8	2.8
47.000	69.42	61.753	10000	22.4	1.623E-3	168.000	20.13	86.77	0.2320	6.613	8653.2100	8.783E-4	10817	1.0817E6	3.384E-3	0.8	2.8
48.012	64.85	54.519	10000	22.4	3.449E-3	169.012	17.77	81.07	0.2192	14.05	8714.7402	2.138E-3	10893	1.0893E6	3.384E-3	0.8	2.8
48.992	60.21	48.802	10000	22.4	1.826E-3	169.992	15.91	75.26	0.2113	7.440	8770.2803	1.313E-3	10963	1.0963E6	3.383E-3	0.8	2.8
50.016	53.77	39.899	10000	22.4	3.652E-3	171.016	13.00	67.21	0.1935	14.88	8844.5898	3.294E-3	11056	1.1056E6	3.384E-3	0.8	2.9
51.016	49.03	33.876	10000	22.4	2.435E-3	172.016	11.04	61.28	0.1802	9.920	8893.4502	2.641E-3	11117	1.1117E6	3.384E-3	0.9	2.9
51.996	44.14	29.997	10000	22.4	3.043E-3	172.996	9.777	55.18	0.1772	12.40	8936.3398	4.073E-3	11170	1.1170E6	3.384E-3	0.9	2.9
52.996	39.80	25.348	10000	22.4	5.072E-3	173.996	8.262	49.75	0.1661	20.67	8973.3799	8.350E-3	11217	1.1217E6	3.384E-3	0.9	2.9
54.012	34.95	20.005	10000	22.4	7.710E-3	175.012	6.521	43.68	0.1493	31.41	9009.9404	0.01646	11262	1.1262E6	3.383E-3	0.9	2.9
54.996	29.86	15.394	10000	22.4	7.710E-3	175.996	5.018	37.33	0.1344	31.41	9039.8896	0.02255	11300	1.1300E6	3.384E-3	0.9	2.9
56.020	25.52	11.654	10000	22.4	7.507E-3	177.020	3.798	31.90	0.1191	30.59	9064.0303	0.03005	11330	1.1330E6	3.384E-3	0.9	3.0
57.016	20.36	7.7425	10000	22.4	3.449E-3	178.016	2.524	25.45	0.09915	14.05	9087.7002	0.02169	11360	1.1360E6	3.383E-3	1.0	3.0
57.996	14.63	4.5488	10000	22.4	7.101E-3	178.996	1.483	18.29	0.08106	28.93	9105.1797	0.08648	11381	1.1381E6	3.383E-3	1.0	3.0
58.992	9.950	2.4044	10000	22.4	7.507E-3	179.992	0.7837	12.44	0.06301	30.59	9116.4600	0.1977	11396	1.1396E6	3.383E-3	1.0	3.0
60.000	6.728	1.1338	10000	22.4	7.101E-3	181.000	0.3696	8.409	0.04395	28.93	9121.3896	0.4091	11402	1.1402E6	3.383E-3	1.0	3.0

